N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide

Base Information

• Chemical Name: N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide
• CAS No.: 1204187-46-1
• Molecular Formula: C₂₈H₂₉N₃O₆
• Molecular Weight: 503.555

Synonyms:N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide

Chemical Property of N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide

Chemical Property:

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Technology Process of N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide

There total 1 articles about N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N1,N3-di((S)-benzyl-methoxycarbonylmethyl)-5-nitro-1,3-benzene dicarboxyamide (1204187-44-9) → N1,N3-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide (1204187-46-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1039/b914770e

Reference yield:

N1,N3-di((S)-benzyl-methoxycarbonylmethyl)-5-amino-1,3-benzene dicarboxyamide (1204187-46-1) + 2,2'-bipyridyl-4,4'-dicarboxylic acid chloride (72460-28-7) → 4,4'-bis{(N1,N3-di((S)-benzyl-methoxycarbonylmethyl)-1,3-benzene dicarboxyamide-5-aminocarbonyl)}-2,2'-bipyridine (1204187-48-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Reflux;

DOI:10.1039/b914770e

upstream raw materials:

N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-5-nitro-1,3-benzene dicarboxyamide

Downstream raw materials:

4,4'-bis{(N₁,N₃-di((S)-benzyl-methoxycarbonylmethyl)-1,3-benzene dicarboxyamide-5-aminocarbonyl)}-2,2'-bipyridine

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