Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

Base Information

Chemical Name:Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester
CAS No.:162048-70-6
Molecular Formula:C₂₂H₃₂O₂S₂
Molecular Weight:392.627
Hs Code.:

Synonyms:Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

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Chemical Property of Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

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Technology Process of Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

There total 3 articles about Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 140-89-6
potassium ethyl xanthogenate

: 162048-67-1
2-Bromo-2-(4-pentyl-cyclohexyl)-1-phenyl-ethanone

: 162048-70-6
Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1039/DT9950000587

Reference yield:

: 162048-83-1
(4-Pentylcyclohexyl)ethanoyl chloride

: 162048-70-6
Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / AlCl₃ / CH₂Cl₂ / 18 h

2: 88 percent / Br₂ / CH₂Cl₂ / 1.) r.t., 1 h, 2.) reflux, 6 h

3: 82 percent / ethanol / 2 h / Heating

With aluminium trichloride; bromine; In ethanol; dichloromethane;
DOI:10.1039/DT9950000587

Reference yield:

: 74603-16-0
1-trans(4-t-pentylcyclohexyl)acetic acid

: 162048-70-6
Dithiocarbonic acid O-ethyl ester S-[2-oxo-1-(4-pentyl-cyclohexyl)-2-phenyl-ethyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / SOCl₂ / 1.) r.t., 20 min, 2.) reflux, 4 h

2: 80 percent / AlCl₃ / CH₂Cl₂ / 18 h

3: 88 percent / Br₂ / CH₂Cl₂ / 1.) r.t., 1 h, 2.) reflux, 6 h

4: 82 percent / ethanol / 2 h / Heating

With aluminium trichloride; thionyl chloride; bromine; In ethanol; dichloromethane;
DOI:10.1039/DT9950000587