C₂₉H₃₈O₈

Base Information

• Chemical Name: C₂₉H₃₈O₈
• CAS No.: 159012-52-9
• Molecular Formula: C₂₉H₃₈O₈
• Molecular Weight: 514.616
• Mol file: 159012-52-9.mol

Synonyms:C₂₉H₃₈O₈

Chemical Property of C₂₉H₃₈O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₈O₈

There total 4 articles about C₂₉H₃₈O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

13-acetyl-9-dihydrobaccatin III (142203-65-4) → C29H38O8 (159012-52-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 72 percent / lithium hexamethyldisilazide (LiHMDS) / tetrahydrofuran / -78 °C

2: 95 percent / Bu₃SnH, AIBN / toluene

3: 88 percent / DMAP / toluene

4: 94 percent / Bu₃SnH, AIBN / toluene

5: CH₃Li / tetrahydrofuran

With dmap; 2,2'-azobis(isobutyronitrile); methyllithium; tri-n-butyl-tin hydride; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;

DOI:10.1016/S0040-4039(00)76947-4

Reference yield:

9-deoxo-13-acetylbaccatin III (159012-46-1) → C29H38O8 (159012-52-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / DMAP / toluene

2: 94 percent / Bu₃SnH, AIBN / toluene

3: CH₃Li / tetrahydrofuran

With dmap; 2,2'-azobis(isobutyronitrile); methyllithium; tri-n-butyl-tin hydride; In tetrahydrofuran; toluene;

DOI:10.1016/S0040-4039(00)76947-4

Reference yield:

C35H44O12S2 (159012-45-0) → C29H38O8 (159012-52-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 95 percent / Bu₃SnH, AIBN / toluene

2: 88 percent / DMAP / toluene

3: 94 percent / Bu₃SnH, AIBN / toluene

4: CH₃Li / tetrahydrofuran

With dmap; 2,2'-azobis(isobutyronitrile); methyllithium; tri-n-butyl-tin hydride; In tetrahydrofuran; toluene;

DOI:10.1016/S0040-4039(00)76947-4

upstream raw materials:

13-acetyl-9-dihydrobaccatin III

9-deoxo-13-acetylbaccatin III

C₃₅H₄₄O₁₂S₂

C₃₇H₄₄N₂O₁₁S

Downstream raw materials:

C₃₃H₄₀N₂O₈S

C₂₉H₃₈O₇