[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

Base Information

Chemical Name:[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol
CAS No.:1246924-59-3
Molecular Formula:C₁₇H₂₅NO₃Si
Molecular Weight:319.476
Hs Code.:

Synonyms:[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

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Technology Process of [5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

There total 1 articles about [5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1246924-58-2
5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazole-4-carboxylic acid ethyl ester

: 1246924-59-3
[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

Guidance literature:: 5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazole-4-carboxylic acid ethyl ester; With lithium borohydride; In tetrahydrofuran; Reflux;

With water; Rochelle's salt; In tetrahydrofuran; for 1h;

Reference yield: 47.0%

: 73781-91-6
6-Chloronicotinic acid methyl ester

: 1246924-59-3
[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol

: 1246924-60-6
6-[5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-ylmethoxy]-nicotinic acid methyl ester

Guidance literature:: [5-(tert-butyl-dimethyl-silanyloxymethyl)-3-phenyl-isoxazol-4-yl]-methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃;

6-Chloronicotinic acid methyl ester; In tetrahydrofuran; mineral oil; at 20 ℃; Cooling with ice;