2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

Base Information

Chemical Name:2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde
CAS No.:1447768-80-0
Molecular Formula:C₁₉H₁₁F₄OP
Molecular Weight:362.263
Hs Code.:

Synonyms:2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

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Chemical Property of 2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

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Technology Process of 2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

There total 4 articles about 2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 27384-33-4
(2-bromo-3,4,5,6-tetrafluorophenyl)diphenylphosphine

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1447768-80-0
2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

Guidance literature:: (2-bromo-3,4,5,6-tetrafluorophenyl)diphenylphosphine; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

N,N-dimethyl-formamide; In diethyl ether; hexane; at -50 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00679

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1447768-80-0
2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / Inert atmosphere; Schlenk technique

1.2: Inert atmosphere; Schlenk technique

2.1: n-butyllithium / hexane; diethyl ether / 0.25 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/om4004303

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 1447768-80-0
2-(diphenylphosphaneyl)-3,4,5,6-tetrafluorobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / Inert atmosphere; Schlenk technique

1.2: Inert atmosphere; Schlenk technique

2.1: n-butyllithium / hexane; diethyl ether / 0.25 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/om4004303