Technology Process of C12H16ClNO3*ClH
There total 3 articles about C12H16ClNO3*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C12H14ClNO5;
With
thiophene; hydrogen;
platinum on activated charcoal; vanadia;
In
tetrahydrofuran; di-isopropyl ether;
at 20 ℃;
for 20h;
With
hydrogenchloride;
In
tetrahydrofuran; ethanol; di-isopropyl ether; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl acetamide / 16 h / 60 °C
2: thiophene; hydrogen / platinum on activated charcoal; vanadia / tetrahydrofuran; di-isopropyl ether / 20 h / 20 °C
With
thiophene; hydrogen; potassium carbonate;
platinum on activated charcoal; vanadia;
In
tetrahydrofuran; di-isopropyl ether; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl acetamide / 16 h / 60 °C
2: thiophene; hydrogen / platinum on activated charcoal; vanadia / tetrahydrofuran; di-isopropyl ether / 20 h / 20 °C
With
thiophene; hydrogen; potassium carbonate;
platinum on activated charcoal; vanadia;
In
tetrahydrofuran; di-isopropyl ether; N,N-dimethyl acetamide;