2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester

Base Information

• Chemical Name: 2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester
• CAS No.: 1188329-19-2
• Molecular Formula: C₁₀H₁₆O₃
• Molecular Weight: 184.235
• Mol file: 1188329-19-2.mol

Synonyms:2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester

Chemical Property of 2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester

There total 1 articles about 2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyllithium (917-54-4) + 4-Methyl-2-carbomethoxy-2-cyclohexenone (132117-95-4) → 2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester (1188329-19-2)

Guidance literature:

With copper(l) iodide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

DOI:10.1039/b905910e

Reference yield: 91.0%

2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester (1188329-19-2) → 2,3-dimethyl-6-oxocyclohex-1-enecarboxylic acid methyl ester (1188329-20-5)

Guidance literature:

2,3-dimethyl-6-oxocyclohexanecarboxylic acid methyl ester; With pyridine; Phenylselenyl chloride; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;

With dihydrogen peroxide; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/b905910e

upstream raw materials:

methyllithium

4-Methyl-2-carbomethoxy-2-cyclohexenone

Downstream raw materials:

2,3-dimethyl-6-oxocyclohex-1-enecarboxylic acid methyl ester