4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester

Base Information

• Chemical Name: 4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester
• CAS No.: 643013-03-0
• Molecular Formula: C₁₇H₁₅F₃N₂O₂S
• Molecular Weight: 368.38

Synonyms:4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester

Chemical Property of 4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester

Chemical Property:

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Technology Process of 4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester

There total 1 articles about 4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

[(4-trifluoromethylphenyl)-(4-methoxycarbonylbenzyl)thiocarbamoyl]carbamic acid 9H-fluoren-9-ylmethyl ester (643013-00-7) → 4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester (643013-03-0)

Guidance literature:

With piperidine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

4-[1-(4-trifluoromethylphenyl)thioureidomethyl]benzoic acid methyl ester (643013-03-0) + 4-chlorobenzoylmethyl bromide (536-38-9) → 4-{[[4-(4-chlorophenyl)thiazol-2-yl]-(4-trifluoromethylphenyl)amino]methyl}benzoic acid methyl ester (643013-15-4)

Guidance literature:

With acetic acid; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1021/jm8016249

upstream raw materials:

[(4-trifluoromethylphenyl)-(4-methoxycarbonylbenzyl)thiocarbamoyl]carbamic acid 9H-fluoren-9-ylmethyl ester

Downstream raw materials:

4-{[[4-(4-chlorophenyl)thiazol-2-yl]-(4-trifluoromethylphenyl)amino]methyl}benzoic acid methyl ester

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