C₁₈H₂₆O₄

Base Information

Chemical Name:C₁₈H₂₆O₄
CAS No.:1616868-93-9
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:

C<sub>18</sub>H<sub>26</sub>O<sub>4</sub>

Synonyms:C₁₈H₂₆O₄

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Chemical Property of C₁₈H₂₆O₄

Chemical Property:

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Technology Process of C₁₈H₂₆O₄

There total 9 articles about C₁₈H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1616868-92-8
(E)-ethyl 5-((4R,5R)-5-((benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)pent-2-enoate

: 1616868-93-9
C₁₈H₂₆O₄

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -20 - 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2014.02.096

Reference yield:

: 78469-77-9
1-O-benzyl-2,3-O-isopropylidene-D-threitol

: 1616868-93-9
C₁₈H₂₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / -78 °C

2: benzene / 6 h / 20 °C

3: nickel(II) chloride hexahydrate; sodium tetrahydroborate; methanol / 0 - 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

5: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / -78 °C

6: benzene / 6 h / 20 °C

7: diisobutylaluminium hydride / dichloromethane / 2 h / -20 - 20 °C

With methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; oxalyl dichloride; nickel(II) chloride hexahydrate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; benzene; 1: |Swern Oxidation / 5: |Swern Oxidation;
DOI:10.1016/j.tetlet.2014.02.096

Reference yield:

: 1616868-90-6
C₁₈H₂₆O₅

: 1616868-93-9
C₁₈H₂₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / -78 °C

3: benzene / 6 h / 20 °C

4: diisobutylaluminium hydride / dichloromethane / 2 h / -20 - 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; benzene; 2: |Swern Oxidation;
DOI:10.1016/j.tetlet.2014.02.096