6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

Base Information

Chemical Name:6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine
CAS No.:482615-23-6
Molecular Formula:C₂₁H₃₀N₆O
Molecular Weight:382.509
Hs Code.:

Synonyms:6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

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Chemical Property of 6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

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Technology Process of 6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

There total 5 articles about 6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 482615-52-1
N-benzyl-2-fluoro-9-isopropyl-purin-6-amine

: 74608-29-0
(3S)-3-amino-2-methyl-pentan-2-ol

: 482615-23-6
6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; butan-1-ol; at 140 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.08.051

Reference yield:

: 3800-23-5
N-benzyl-2-fluoro-9H-purin-6-amine

: 482615-23-6
6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 2,4-dichlorophenoxyacetic acid dimethylamine / 48 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; butan-1-ol / 72 h / 140 °C / Inert atmosphere

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In 2,4-dichlorophenoxyacetic acid dimethylamine; dimethyl sulfoxide; butan-1-ol;
DOI:10.1016/j.bmc.2011.08.051

Reference yield:

: (3R)-2-methyl-3-(trityl-amino)-pentan-2-ol

: 482615-23-6
6-benzylamino-2-[(1S)-1-ethyl-2-hydroxy-2-methylpropylamino]-9-isopropylpurine

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide; butan-1-ol / 72 h / 140 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; butan-1-ol;
DOI:10.1016/j.bmc.2011.08.051