4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

Base Information

Chemical Name:4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate
CAS No.:1306616-33-0
Molecular Formula:C₁₉H₂₄F₆O₈S₂
Molecular Weight:558.517
Hs Code.:

Synonyms:4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

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Chemical Property of 4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

Chemical Property:

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Technology Process of 4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

There total 4 articles about 4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1306616-32-9
4-methyl-2-(2-methylpropyl)-pentyl 3,5-dihydroxybenzoate

: 1306616-33-0
4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

Guidance literature:: In pyridine; at 20 ℃; for 3h; Cooling;
DOI:10.1021/jo200658q

Reference yield:

: 60302-31-0
4-methyl-2-(2-methylpropyl)-pentanoic acid ethyl ester

: 1306616-33-0
4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -100 - 0 °C / Inert atmosphere

2: sulfuric acid / 1,4-dioxane / Inert atmosphere; Reflux

3: pyridine / 3 h / 20 °C / Cooling

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; pyridine;
DOI:10.1021/jo200658q

Reference yield:

: 81749-14-6
diethyl 2,2-bis(2-methylpropyl)propanedionate

: 1306616-33-0
4-methyl-2-(2-methylpropyl)pentyl 3,5-bis(trifluoromethanesulfonyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: water; lithium chloride / dimethyl sulfoxide / 24 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -100 - 0 °C / Inert atmosphere

3: sulfuric acid / 1,4-dioxane / Inert atmosphere; Reflux

4: pyridine / 3 h / 20 °C / Cooling

With lithium aluminium tetrahydride; sulfuric acid; water; lithium chloride; In tetrahydrofuran; 1,4-dioxane; pyridine; dimethyl sulfoxide;
DOI:10.1021/jo200658q