1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

Base Information

Chemical Name:1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate
CAS No.:1007131-28-3
Molecular Formula:BF₄*C₁₅H₁₇O₃S₂
Molecular Weight:396.235
Hs Code.:

Synonyms:1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

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Chemical Property of 1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

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Technology Process of 1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

There total 1 articles about 1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 110-01-0
thiophene

: 1007131-26-1
2-(bromomethyl)-5-(phenylsulfonyl)furan

: 1007131-28-3
1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

Guidance literature:: With aqueous sodium tetrafluoroborate; In dichloromethane; at 20 ℃; for 168h;
DOI:10.1039/b713447a

Reference yield:

: 1007131-28-3
1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 1007131-35-2
(1R,2S)-1-[5-(phenylsulfonyl)-2-furyl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]oxirane

: 900144-17-4
(1R,2R)-1-[5-(phenylsulfonyl)-2-furyl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]oxirane

: 900144-15-2
(1S,2R)-1-[5-(phenylsulfonyl)-2-furyl]-2-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]oxirane

Guidance literature:: 1-{[(5-phenylsulfonyl)-2-furyl]methyl}tetrahydrothiophenium tetrafluoroborate; With potassium hexamethylsilazane; In dichloromethane;

2,3-isopropylidene-glyceraldehyde; In dichloromethane; at -78 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1039/b713447a