Technology Process of C13H19NO6S
There total 6 articles about C13H19NO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; ammonium formate;
In
methanol;
at 20 - 40 ℃;
for 8h;
Inert atmosphere;
DOI:10.3998/ark.5550190.0013.319
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ammonium chloride / pentane; diethyl ether / 16 h / 0 - 23 °C / Inert atmosphere
2: hydrogenchloride / water; ethanol / 2 h / 90 °C / Inert atmosphere
3: triethylamine; triethylamine sulfur trioxide / dichloromethane / 48 h / 20 - 23 °C / Inert atmosphere
4: sodium tetrahydroborate / methanol / 16 h / 20 - 23 °C / Inert atmosphere
5: 5%-palladium/activated carbon; ammonium formate / methanol / 8 h / 20 - 40 °C / Inert atmosphere
With
hydrogenchloride; sodium tetrahydroborate; 5%-palladium/activated carbon; ammonium formate; triethylamine sulfur trioxide; ammonium chloride; triethylamine;
In
methanol; diethyl ether; ethanol; dichloromethane; water; pentane;
DOI:10.3998/ark.5550190.0013.319
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / water; ethanol / 2 h / 90 °C / Inert atmosphere
2: triethylamine; triethylamine sulfur trioxide / dichloromethane / 48 h / 20 - 23 °C / Inert atmosphere
3: sodium tetrahydroborate / methanol / 16 h / 20 - 23 °C / Inert atmosphere
4: 5%-palladium/activated carbon; ammonium formate / methanol / 8 h / 20 - 40 °C / Inert atmosphere
With
hydrogenchloride; sodium tetrahydroborate; 5%-palladium/activated carbon; ammonium formate; triethylamine sulfur trioxide; triethylamine;
In
methanol; ethanol; dichloromethane; water;
DOI:10.3998/ark.5550190.0013.319