Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

Base Information

Chemical Name:Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)
CAS No.:1210067-70-1
Molecular Formula:Au*C₁₃H₁₁N₂OS
Molecular Weight:440.276
Hs Code.:

Au<sup>(1+)</sup>*SC<sub>6</sub>H<sub>4</sub>NHCONHC<sub>6</sub>H<sub>5</sub><sup>(1-)</sup>=Au(SC<sub>6</sub>H<sub>4</sub>NHCONHC<sub>6</sub>H<sub>5</sub>)

Synonyms:Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

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Chemical Property of Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

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Technology Process of Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

There total 1 articles about Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 13682-61-6
potassium tetrachloroaurate(III)

: 943414-53-7
HSC₆H₄NHCONHC₆H₅

: 1210067-70-1
Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

Guidance literature:: With 2,2'-thiodiethanol; In methanol; H₂O; tetrahydrofuran; under N2; 2,2'-thiodiethanol added dropwise to soln. of KAuCl4 in MeOH-H2O; stirred; ligand in THF added; stirred for 30 min; ppt. sepd.; washed with H2O, MeOH and Et2O; dried under vac.; elem. anal.;
DOI:10.1021/ic9021068

Reference yield: 80.0%

: 60-29-7,927820-24-4
diethyl ether

: 1210067-70-1
Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

: 603-35-0
triphenylphosphine

: [(C₅H₅NHCONHC₆H₄S)Au(triphenylphosphine)]*0.5(diethyl ether)

Guidance literature:: In CH₂Cl₂; under N2; mixt. of Au complex and phosphine in CH2Cl2 stirred for 2 h; filtered; solvent removed under reduced pressure; dissolved in CH2Cl2; recrystd. by diffusion of Et2O vapor into CH2Cl2 soln.; elem. anal.;
DOI:10.1021/ic9021068

Reference yield: 65.0%

: 60-29-7,927820-24-4
diethyl ether

: 1210067-70-1
Au⁽¹⁺⁾*SC₆H₄NHCONHC₆H₅^(1-)=Au(SC₆H₄NHCONHC₆H₅)

: 107163-51-9
17-diphenylphosphino-2,5,8,11,14-pentaoxa-bicyclo<13.4.0>-nonadeca-15,17,19-triene

: [(C₅H₅NHCONHC₆H₄S)Au(4'-diphenylphosphinobenzo-15-crown-5)]*(diethyl ether)

Guidance literature:: In CH₂Cl₂; under N2; mixt. of Au complex and phosphine in CH2Cl2 stirred for 2 h; filtered; solvent removed under reduced pressure; dissolved in CH2Cl2; recrystd. by layering n-hexane onto CH2Cl2 soln.; solid washed with Et2O;elem. anal.;
DOI:10.1021/ic9021068