C₄₄H₈₀O₁₃Si₃

Base Information

Chemical Name:C₄₄H₈₀O₁₃Si₃
CAS No.:1095272-69-7
Molecular Formula:C₄₄H₈₀O₁₃Si₃
Molecular Weight:901.368
Hs Code.:

C<sub>44</sub>H<sub>80</sub>O<sub>13</sub>Si<sub>3</sub>

Synonyms:C₄₄H₈₀O₁₃Si₃

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Chemical Property of C₄₄H₈₀O₁₃Si₃

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Technology Process of C₄₄H₈₀O₁₃Si₃

There total 24 articles about C₄₄H₈₀O₁₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1095272-58-4
C₂₁H₄₀O₆Si

: 1095272-57-3
C₂₃H₄₀O₇Si₂

: 1095272-69-7
C₄₄H₈₀O₁₃Si₃

Guidance literature:: C₂₁H₄₀O₆Si; With phenylborondichloride; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 0 ℃; for 2.16667h; Inert atmosphere;

C₂₃H₄₀O₇Si₂; In dichloromethane; at -78 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/jo400260m

Reference yield:

: 1095272-57-3
C₂₃H₄₀O₇Si₂

: C₂₇H₄₄BClO₆Si

: 1095272-69-7
C₄₄H₈₀O₁₃Si₃

Guidance literature:: In dichloromethane; at -78 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/ol802466t

Reference yield:

: C₂₀H₃₈O₆Si

: 1095272-69-7
C₄₄H₈₀O₁₃Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 2 h / Inert atmosphere

2.1: dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: phenylborondichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.2: 2.17 h / -78 - 0 °C / Inert atmosphere

3.3: 1.25 h / -78 °C / Inert atmosphere

With camphor-10-sulfonic acid; phenylborondichloride; In dichloromethane;
DOI:10.1021/jo400260m