C₃₆H₃₃N₃O₇

Base Information

Chemical Name:C₃₆H₃₃N₃O₇
CAS No.:188028-00-4
Molecular Formula:C₃₆H₃₃N₃O₇
Molecular Weight:619.674
Hs Code.:

C<sub>36</sub>H<sub>33</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₆H₃₃N₃O₇

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Chemical Property of C₃₆H₃₃N₃O₇

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Technology Process of C₃₆H₃₃N₃O₇

There total 8 articles about C₃₆H₃₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 188028-28-6
C₃₆H₃₁N₃O₅

: 188028-00-4
C₃₆H₃₃N₃O₇

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; for 16h;
DOI:10.1021/ja971304x

Reference yield:

: 188028-91-3
C₃₆H₃₁N₃O₇

: 188028-00-4
C₃₆H₃₃N₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / LiBH₄ / tetrahydrofuran / 0.33 h

2: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature

3: 85 percent / BF₃*OEt₂ / diethyl ether / 24 h / 25 - 30 °C

4: 95 percent / NaBH₄ / methanol; CH₂Cl₂; CHCl₃ / 0.08 h

5: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min

6: 88 percent / Martin's sulfurane / CDCl₃ / 0.33 h

7: 84 percent / 4-methylmorpholine-N-oxide, OsO₄ / 2-methyl-propan-2-ol; acetone; H₂O / 16 h

With sodium tetrahydroborate; osmium(VIII) oxide; lithium borohydride; Martins sulfurane; boron trifluoride diethyl etherate; pyridinium trifluroacetate; sodium hydride; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; chloroform-d1; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone; tert-butyl alcohol; benzene;
DOI:10.1021/ja971304x

Reference yield:

: 188028-23-1
C₃₅H₃₁N₃O₆

: 188028-00-4
C₃₆H₃₃N₃O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature

2: 85 percent / BF₃*OEt₂ / diethyl ether / 24 h / 25 - 30 °C

3: 95 percent / NaBH₄ / methanol; CH₂Cl₂; CHCl₃ / 0.08 h

4: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min

5: 88 percent / Martin's sulfurane / CDCl₃ / 0.33 h

6: 84 percent / 4-methylmorpholine-N-oxide, OsO₄ / 2-methyl-propan-2-ol; acetone; H₂O / 16 h

With sodium tetrahydroborate; osmium(VIII) oxide; Martins sulfurane; boron trifluoride diethyl etherate; pyridinium trifluroacetate; sodium hydride; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; In methanol; diethyl ether; chloroform-d1; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone; tert-butyl alcohol; benzene;
DOI:10.1021/ja971304x