(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Chemical Name:(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride
CAS No.:1269473-20-2
Molecular Formula:C₂₇H₃₁N₄O*Cl
Molecular Weight:463.022
Hs Code.:

Synonyms:(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Chemical Property of (S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Technology Process of (S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

There total 8 articles about (S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 2108-54-5
1-(4-methoxyphenyl)pentane-1,4-dione

: 1269473-12-2
(S)-5-(aminomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

: 1269473-20-2
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; at 50 ℃; Inert atmosphere;
DOI:10.1002/asia.201000617

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1269473-20-2
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / 0 °C

2: sodium azide / N,N-dimethyl-formamide / 80 °C

3: dichloromethane / 17 h / 23 °C / Inert atmosphere

4: methanol / 2 h / 50 °C

5: hydrogenchloride; chlorobenzene / 1,4-dioxane / 0.83 h / 100 °C / Inert atmosphere

6: ammonium chloride; zinc / ethanol; water / 1 h / 20 °C

7: hydrogenchloride / 1,4-dioxane; methanol / 50 °C / Inert atmosphere

With hydrogenchloride; sodium azide; ammonium chloride; triethylamine; chlorobenzene; zinc; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 7: Paal-Knorr pyrrole synthesis;
DOI:10.1002/asia.201000617

Reference yield:

: 1269473-11-1
(S)-5-(azidomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

: 1269473-20-2
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-5-methyl-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5Hpyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; zinc / ethanol; water / 1 h / 20 °C

2: hydrogenchloride / 1,4-dioxane; methanol / 50 °C / Inert atmosphere

With hydrogenchloride; ammonium chloride; zinc; In 1,4-dioxane; methanol; ethanol; water; 2: Paal-Knorr pyrrole synthesis;
DOI:10.1002/asia.201000617