N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

Base Information

Chemical Name:N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide
CAS No.:310896-78-7
Molecular Formula:C₁₉H₂₇NOSi₂
Molecular Weight:341.6
Hs Code.:

Synonyms:N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

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Technology Process of N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

There total 3 articles about N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 66224-70-2
3-(trimethylsilyl)propynoyl chloride

: 101911-12-0
6,6-dimethyl-1-phenyl-2-aza-6-sila-4-heptyne

: 310896-78-7
N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

Guidance literature:: DOI:10.1021/ol0065221

Reference yield:

: 1197-51-9
N-propargylbenzylamine

: 310896-78-7
N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / BuLi

2: 80 percent

With n-butyllithium; 1: silylation / 2: Acylation;
DOI:10.1021/ol0065221

Reference yield:

: 100-46-9
benzylamine

: 310896-78-7
N-benzyl-N-[3-(trimethylsilyl)-2-propynyl]-3-(trimethylsilyl)-2-propynamide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃

2: 72 percent / BuLi

3: 80 percent

With n-butyllithium; potassium carbonate; 1: Substitution / 2: silylation / 3: Acylation;
DOI:10.1021/ol0065221