(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

Base Information

Chemical Name:(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate
CAS No.:1026429-34-4
Molecular Formula:C₂₅H₂₃Cl₂NO₄S
Molecular Weight:504.434
Hs Code.:

Synonyms:(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

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Chemical Property of (E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

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Technology Process of (E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

There total 8 articles about (E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24966-39-0
2,6-dichlorothiophenol

: (E)-3-{6-Chloromethyl-3-[2-(4-methoxy-phenyl)-ethoxy]-pyridin-2-yl}-acrylic acid methyl ester; hydrochloride

: 1026429-34-4
(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 50 ℃;
DOI:10.1021/jm960248s

Reference yield:

: 66497-42-5
3-hydroxy-6-methylpicolinaldehyde

: 1026429-34-4
(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / toluene / 0.5 h / 50 °C

2: Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3: MCPBA / CH₂Cl₂ / Ambient temperature

4: trifluoroacetic anhydride / dimethylformamide / Ambient temperature

5: SOCl₂ / toluene

6: DBU / acetonitrile / 50 °C

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic anhydride; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm960248s

Reference yield:

: 702-23-8
2-(4-Methoxyphenyl)ethanol

: 1026429-34-4
(E)-methyl 3-[3-[2-(4-methoxyphenyl)ethyloxy]-6-[(2,6-dichlorophenylthio)-methyl]-2-pyridinyl]-2-propenoate

Guidance literature:: Multi-step reaction with 5 steps

1: Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: MCPBA / CH₂Cl₂ / Ambient temperature

3: trifluoroacetic anhydride / dimethylformamide / Ambient temperature

4: SOCl₂ / toluene

5: DBU / acetonitrile / 50 °C

With thionyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic anhydride; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm960248s