[2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

Base Information

Chemical Name:[2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate
CAS No.:1456712-13-2
Molecular Formula:C₁₈H₂₃N₅O₉S₂
Molecular Weight:517.541
Hs Code.:

Synonyms:[2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

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Chemical Property of [2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

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Technology Process of [2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

There total 2 articles about [2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1456712-17-6
1-(4,6-dimethoxypyrimidin-2-yl)-3-[2-(hydroxymethyl)-5-(methanesulfonamidomethyl)phenyl]sulfonyl-urea

: 108-24-7
acetic anhydride

: 1456712-13-2
[2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 23h;

Reference yield:

: 208465-21-8
mesosulfuron-methyl

: 1456712-13-2
[2-[(4,6-dimethoxypyrimidin-2-yl)carbamoylsulfamoyl]-4-(methanesulfonamidomethyl)phenyl]methylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -20 - 20 °C

2: triethylamine / dichloromethane / 23 h / 20 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;