2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

Base Information

Chemical Name:2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside
CAS No.:81823-03-2
Molecular Formula:C₄₉H₄₈N₂O₁₁S
Molecular Weight:872.993
Hs Code.:

Synonyms:2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

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Chemical Property of 2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

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Technology Process of 2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

There total 4 articles about 2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20672-66-6,40246-26-2,84926-76-1,114179-79-2,115184-49-1
3,4,6-tri-O-benzyl-D-glucopyranose

: 81823-03-2
2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / Ambient temperature

2: hydrogen chloride / diethyl ether / 24 h / Ambient temperature

3: acetonitrile / 0.25 h / Ambient temperature

4: acetonitrile / 24 h / Ambient temperature; in the dark

With pyridine; hydrogenchloride; In diethyl ether; acetonitrile;
DOI:10.1016/S0008-6215(00)88056-8

Reference yield:

: 81823-01-0
3,4,6-tri-O-benzyl-1,2-di-O-p-nitrobenzoyl-D-glucopyranose

: 81823-03-2
2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen chloride / diethyl ether / 24 h / Ambient temperature

2: acetonitrile / 0.25 h / Ambient temperature

3: acetonitrile / 24 h / Ambient temperature; in the dark

With hydrogenchloride; In diethyl ether; acetonitrile;
DOI:10.1016/S0008-6215(00)88056-8

Reference yield:

: 81823-02-1
3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-glucopyranosyl chloride

: 81823-03-2
2-<4-(p-toluenesulfonamido)phenyl>ethyl 3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-glycopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 0.25 h / Ambient temperature

2: acetonitrile / 24 h / Ambient temperature; in the dark

In acetonitrile;
DOI:10.1016/S0008-6215(00)88056-8