(3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

Base Information

Chemical Name:(3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone
CAS No.:214210-36-3
Molecular Formula:C₁₉H₃₀O₂Si
Molecular Weight:318.531
Hs Code.:

Synonyms:(3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

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Chemical Property of (3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

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Technology Process of (3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

There total 8 articles about (3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 768-33-2
phenyldimethylsilyl chloride

: 98587-10-1
(S)-3-n-butyl-5-methylfuran-2(5H)-one

: 214210-36-3
(3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

Guidance literature:: phenyldimethylsilyl chloride; With lithium; In tetrahydrofuran; at 0 ℃; for 16h; Inert atmosphere;

With copper(l) cyanide; In tetrahydrofuran; at -70 - 0 ℃; for 0.333333h; Inert atmosphere;

(S)-3-n-butyl-5-methylfuran-2(5H)-one; In tetrahydrofuran; at -70 ℃; for 0.333333h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.09.074 DOI:10.1016/j.tet.2012.09.074

Reference yield: 82.0%

: 1262286-20-3
(S)-3-n-hexyl-5-methylfuran-2(5H)-one

: 110769-32-9
(PhMe₂Si)2CuCNLi₂

: 214210-36-3
(3S,4R,5S)-4-(dimethylphenylsilyl)-3-hexyl-4,5-dihydro-5-methyl-2(3H)-furanone

Guidance literature:: (S)-3-n-hexyl-5-methylfuran-2(5H)-one; (PhMe₂Si)2CuCNLi₂; at 70 ℃;

diastereoselective reaction; Acidic conditions;
DOI:10.1016/j.tetlet.2010.10.089