3-Hydroxycard-20(22)-enolide

Base Information

• Chemical Name: 3-Hydroxycard-20(22)-enolide
• CAS No.: 5672-23-1
• Molecular Formula: C₂₃H₃₄O₃
• Molecular Weight: 358.521
• NSC Number: 107129
• DSSTox Substance ID: DTXSID90972166

Synonyms:5672-23-1;3-hydroxycard-20(22)-enolide;NSC107129;DTXSID90972166;NSC-107129

Chemical Property of 3-Hydroxycard-20(22)-enolide

Chemical Property:

• Vapor Pressure: 8.41E-13mmHg at 25°C
• Boiling Point: 515.9°Cat760mmHg
• Flash Point: 205.9°C
• Density: 1.147g/cm³
• XLogP3: 5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 358.25079494
• Heavy Atom Count: 26
• Complexity: 639

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC12CCC(CC1CCC3C2CCC4(C3CCC4C5=CC(=O)OC5)C)O

Technology Process of 3-Hydroxycard-20(22)-enolide

There total 9 articles about 3-Hydroxycard-20(22)-enolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 14,16-Dideoxy-17α-gitoxigenin (1616-05-3,1723-16-6,3842-04-4,3940-87-2,4761-89-1,5672-23-1,14622-60-7,22040-77-3,23330-59-8,35881-65-3,51020-49-6,51020-50-9)

Guidance literature:

Dianhydrogitoxigenin, H2-Raney-Nickel, EtOH oder Pd/BaSO4, Eg oder Pd/C, MeOH, EtOH, Eg., Dioxan, AcOEt oder Benzol;

Reference yield:

→ 3β-Hydroxy-5β,14α-card-20(22)-enolid (1616-05-3,1723-16-6,3842-04-4,3940-87-2,4761-89-1,5672-23-1,14622-60-7,22040-77-3,23330-59-8,35881-65-3,51020-49-6,51020-50-9)

Guidance literature:

β-Anhydrodigitoxigenin, H2-Pd/BaSO4, Eg.;

Reference yield:

→ 3β-Hydroxy-5α-card-20(22)-enolid (1616-05-3,1723-16-6,3842-04-4,3940-87-2,4761-89-1,5672-23-1,14622-60-7,22040-77-3,23330-59-8,35881-65-3,51020-49-6,51020-50-9)

Guidance literature:

aus 3a, HCl;

DOI:10.1021/jo00830a031

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