N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

Base Information

Chemical Name:N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide
CAS No.:1046135-19-6
Molecular Formula:C₂₄H₁₂F₁₂N₂S₂
Molecular Weight:620.486
Hs Code.:

N<sub>1</sub>,N<sub>3</sub>-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

Synonyms:N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

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Technology Process of N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

There total 3 articles about N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 181872-56-0
N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarboxamide

: 1046135-19-6
N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

Guidance literature:: With Lawessons reagent; In toluene; for 16h; Reflux; Inert atmosphere;
DOI:10.1002/ejoc.201001439

Reference yield:

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 1046135-19-6
N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / N,N-dimethyl-formamide / 0 - 75 °C

2: Lawessons reagent / toluene / 16 h / Reflux; Inert atmosphere

With Lawessons reagent; dmap; triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201001439

Reference yield:

: 328-74-5
3,5-Bis-(trifluoromethyl)aniline

: 1046135-19-6
N₁,N₃-bis(3,5-bis(trifluoromethyl)phenyl)benzene-1,3-dicarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / N,N-dimethyl-formamide / 0 - 75 °C

2: Lawessons reagent / toluene / 16 h / Reflux; Inert atmosphere

With Lawessons reagent; dmap; triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201001439