N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

Base Information

Chemical Name:N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide
CAS No.:1204430-63-6
Molecular Formula:C₂₀H₂₂N₄O₆
Molecular Weight:414.418
Hs Code.:

Synonyms:N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

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Chemical Property of N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

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Technology Process of N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

There total 8 articles about N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1204430-62-5
N-(4-methoxy-3-nitrophenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

: 1204430-63-6
N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In water; at 80 ℃; for 4h;
DOI:10.1016/j.bmc.2011.03.068

Reference yield:

: 3044-56-2
ethyl trimethoxybenzoyl acetate

: 1204430-63-6
N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / diethyl ether / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 80 °C

3: sodium hydroxide / water / 55 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

5: hydrogenchloride; tin(ll) chloride / water / 4 h / 80 °C

With hydrogenchloride; dmap; N-Bromosuccinimide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tin(ll) chloride; sodium hydroxide; In diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.068

Reference yield:

: 1185728-18-0
C₁₅H₁₈N₂O₆

: 1204430-63-6
N-(3-amino-4-methoxyphenyl)-2-oxo-5-(3,4,5-trimethoxyphenyl)-2,3-dihydro-1H-imidazole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 55 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

3: hydrogenchloride; tin(ll) chloride / water / 4 h / 80 °C

With hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tin(ll) chloride; sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.03.068