N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

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Chemical Name:N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide
CAS No.:1420293-09-9
Molecular Formula:C₂₂H₂₉NO₅
Molecular Weight:387.476
Hs Code.:

Synonyms:N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

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Chemical Property of N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

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Technology Process of N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

There total 2 articles about N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1420292-97-2
4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolane

: 141565-14-2,77486-09-0,77486-10-3
N-(2-methoxy-2-oxoethylidene)-1-phenylmethanamine N-oxide

: 1420293-09-9
N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

Guidance literature:: With tert.-butylhydroperoxide; 1,10-Phenanthroline; Copper(I); benzoate; sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/asia.201200359

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 94059-92-4
6,6-dimethoxyhex-1-yne

: 1420293-09-9
N-benzylidene-2-methoxy-2-oxo-1-(4,4,5,5-tetramethyl-2-(pent-4-yn-1-yl)-1,3-dioxolan-2-yl)ethanamine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / diethyl ether / 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide; 1,10-Phenanthroline; Copper(I); benzoate; sodium hydrogencarbonate / dimethyl sulfoxide / 6 h / 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; 1,10-Phenanthroline; boron trifluoride diethyl etherate; Copper(I); benzoate; sodium hydrogencarbonate; In diethyl ether; dimethyl sulfoxide;
DOI:10.1002/asia.201200359