3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

Base Information

Chemical Name:3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride
CAS No.:1441168-53-1
Molecular Formula:C₁₈H₂₆FN*ClH
Molecular Weight:311.87
Hs Code.:

Synonyms:3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

Chemical Property:

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Technology Process of 3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

There total 9 articles about 3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1441169-68-1
3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline

: 1441168-53-1
3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃; for 2h;

Reference yield:

: 1439355-76-6
1-hydroxy-2,2,5,5-tetramethylcyclohexanecarbonitrile

: 1441168-53-1
3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 2.5 h / -78 - 20 °C / Inert atmosphere

2: acetic acid; sodium cyanoborohydride / methanol / 20 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Cooling with ice

4: hydrogenchloride / diethyl ether / 2 h / 20 °C

With hydrogenchloride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1439355-80-2
3,3,6,6-tetramethylcyclohex-1-enecarbaldehyde

: 1441168-53-1
3-fluoro-N-methyl-N-((3,3,6,6-tetramethylcyclohex-1-enyl)methyl)aniline hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium cyanoborohydride / methanol / 20 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Cooling with ice

3: hydrogenchloride / diethyl ether / 2 h / 20 °C

With hydrogenchloride; sodium hydride; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether; N,N-dimethyl-formamide; mineral oil;