N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide
CAS No.:1407182-28-8
Molecular Formula:C₃₉H₆₀N₂O
Molecular Weight:572.918
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

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Chemical Property of N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

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Technology Process of N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

There total 8 articles about N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₅₈N₂O

: 1407182-28-8
N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

Guidance literature:: With sodium cyanoborohydride; acetic acid; In dichloromethane; toluene; tert-butyl alcohol; at 20 ℃; for 16h;
DOI:10.1039/c2cc36329a

Reference yield:

: N-(2,2-diethoxyethyl)-2,6-diisopropylaniline

: 1407182-28-8
N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2: formic acid / 18 h / 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / toluene; tert-butyl alcohol / 1 h / 100 °C / Inert atmosphere; Microwave irradiation

4: sodium cyanoborohydride; acetic acid / dichloromethane; toluene; tert-butyl alcohol / 16 h / 20 °C

With formic acid; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; In dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1039/c2cc36329a

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1407182-28-8
N-(2,6-diisopropylphenyl)-N-(2-(1,1,7,7-tetraethyl-3,3,5,5-tetramethyl-1,2,3,5,6,7-hexahydros-indacen-4-ylamino)ethyl)formamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / 0 - 20 °C

1.2: 18 h / Inert atmosphere

2.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: formic acid / 18 h / 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / toluene; tert-butyl alcohol / 1 h / 100 °C / Inert atmosphere; Microwave irradiation

5.1: sodium cyanoborohydride; acetic acid / dichloromethane; toluene; tert-butyl alcohol / 16 h / 20 °C

With n-butyllithium; formic acid; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1039/c2cc36329a