C₃₇H₄₁FN₃O₉P

Base Information

Chemical Name:C₃₇H₄₁FN₃O₉P
CAS No.:1445380-68-6
Molecular Formula:C₃₇H₄₁FN₃O₉P
Molecular Weight:721.719
Hs Code.:

C<sub>37</sub>H<sub>41</sub>FN<sub>3</sub>O<sub>9</sub>P

Synonyms:C₃₇H₄₁FN₃O₉P

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Chemical Property of C₃₇H₄₁FN₃O₉P

Chemical Property:

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Technology Process of C₃₇H₄₁FN₃O₉P

There total 16 articles about C₃₇H₄₁FN₃O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 53064-79-2
iodomethyl pivaloate

: 1445380-66-4
C₃₁H₃₁FN₃O₇P

: 1445380-68-6
C₃₇H₄₁FN₃O₉P

Guidance literature:: With pyridine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 53064-79-2
iodomethyl pivaloate

: C₃₁H₃₀FN₃O₇P^(1-)

: 1445380-68-6
C₃₇H₄₁FN₃O₉P

Guidance literature:: With pyridine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1445379-59-8
2’-deoxy-2’-fluoro-3’-O-(tert-butyldimethylsilyl)uridine

: 1445380-68-6
C₃₇H₄₁FN₃O₉P

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 3 h / Reflux

2.1: sodium hydroxide / 1,4-dioxane; water / 2 h / 20 °C

2.2: 0.5 h / 20 °C / pH 7

3.1: pyridine / dichloromethane / 14 h / 0 - 20 °C

4.1: 1H-imidazole / dichloromethane / 14 h / 20 °C

4.2: 15 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 - 0 °C / Inert atmosphere

6.2: 1.5 h / 0 - 20 °C / Inert atmosphere

7.1: Triphenylsilyl chloride; dmap; triethylamine / acetonitrile / 2 h / 20 °C

7.2: 1 h

8.1: palladium on activated charcoal; hydrogen / methanol / 2 h / 20 °C

9.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 20 °C / Inert atmosphere

10.1: 1H-tetrazole / acetonitrile / 1 h / 20 °C / Inert atmosphere

10.2: TBDPH / 1 h

11.1: ammonia / methanol / 2 h / 20 °C

12.1: pyridine; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; 1H-tetrazole; 2,4,6-trimethyl-pyridine; dmap; n-butyllithium; Triphenylsilyl chloride; palladium on activated charcoal; ammonia; hydrogen; Dess-Martin periodane; silver nitrate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;