2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

Base Information

Chemical Name:2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide
CAS No.:81246-02-8
Molecular Formula:C₂₃H₂₀N₂O₄
Molecular Weight:388.423
Hs Code.:

Synonyms:2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

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Chemical Property of 2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

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Technology Process of 2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

There total 1 articles about 2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 941-69-5
N-phenyl-maleimide

: 54732-59-1
N-(methoxycarbonyl)-2-phenyl-1,2-dihydropyridine

: 81246-02-8
2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

Guidance literature:: In dichloromethane; for 60h; Heating;
DOI:10.1021/jo00132a002

Reference yield:

: 81246-02-8
2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

: (1S,2R,6R,7R,9S)-4,9-Diphenyl-4,8-diaza-tricyclo[5.2.2.0^2,6]undec-10-ene-3,5-dione

Guidance literature:: With trimethylsilyl iodide; In chloroform; at 20 - 45 ℃; for 11h;
DOI:10.1021/jo00132a002

Reference yield:

: 81246-02-8
2-(methoxycarbonyl)-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-endo-dicarboxylic acid N-phenylimide

: 60427-41-0
N-acetyl-3-endo-phenyl-2-azabicyclo<2.2.2>oct-7-ene-5,6-dicarboxylic acid N-phenylimide

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl iodide / CHCl₃ / 11 h / 20 - 45 °C

2: aq. KOH / CH₂Cl₂ / 2 h

With potassium hydroxide; trimethylsilyl iodide; In dichloromethane; chloroform;
DOI:10.1021/jo00132a002