(6R,9R)-γ-ionol acetate

Base Information

Chemical Name:(6R,9R)-γ-ionol acetate
CAS No.:315208-24-3
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:

Synonyms:(6R,9R)-γ-ionol acetate

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Chemical Property of (6R,9R)-γ-ionol acetate

Chemical Property:

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Technology Process of (6R,9R)-γ-ionol acetate

There total 8 articles about (6R,9R)-γ-ionol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 108-05-4,9003-20-7
vinyl acetate

: (+/-)-(6RS,9RS)-γ-ionol

: 315208-16-3
(6S,9S)-γ-ionol

: 315208-24-3
(6R,9R)-γ-ionol acetate

Guidance literature:: With Lipase PS (Pseudomonas cepacia); In various solvent(s); at 20 ℃; for 72h;
DOI:10.1002/1522-2675(20001004)83:10<2761::AID-HLCA2761>3.0.CO;2-9

Reference yield:

: 49816-69-5
gamma-ionone

: 315208-24-3
(6R,9R)-γ-ionol acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaBH₄ / methanol

2: 30 percent / pyridine / CH₂Cl₂

3: 94 percent / KOH / methanol / 2 h / Heating

4: 40 percent / lipase PS (Pseudomonas cepacia) / various solvent(s) / 72 h / 20 °C

With pyridine; potassium hydroxide; sodium tetrahydroborate; Lipase PS (Pseudomonas cepacia); In methanol; dichloromethane; 1: Reduction / 2: Acylation / 3: Hydrolysis / 4: Acetylation;
DOI:10.1002/1522-2675(20001004)83:10<2761::AID-HLCA2761>3.0.CO;2-9

Reference yield:

: 432-23-5,4350-73-6
2,2-dimethyl-6-methylenecyclohexane-1-carbaldehyde

: 315208-24-3
(6R,9R)-γ-ionol acetate

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 8 h / Heating

2: 96 percent / NaBH₄ / methanol

3: 30 percent / pyridine / CH₂Cl₂

4: 94 percent / KOH / methanol / 2 h / Heating

5: 40 percent / lipase PS (Pseudomonas cepacia) / various solvent(s) / 72 h / 20 °C

With pyridine; potassium hydroxide; sodium tetrahydroborate; Lipase PS (Pseudomonas cepacia); In methanol; dichloromethane; toluene; 1: Wittig reaction / 2: Reduction / 3: Acylation / 4: Hydrolysis / 5: Acetylation;
DOI:10.1002/1522-2675(20001004)83:10<2761::AID-HLCA2761>3.0.CO;2-9