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C23H30O6

Base Information
  • Chemical Name:C23H30O6
  • CAS No.:1338989-57-3
  • Molecular Formula:C23H30O6
  • Molecular Weight:402.488
  • Hs Code.:
C<sub>23</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:C23H30O6

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Chemical Property of C23H30O6
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Technology Process of C23H30O6

There total 10 articles about C23H30O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 ℃; regioselective reaction;
DOI:10.1016/j.tetlet.2011.08.051
Guidance literature:
Multi-step reaction with 7 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 25 °C
2: tert.-butyl lithium / tetrahydrofuran / -78 °C
3: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C
4: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C
5: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
7: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
With tert.-butylhydroperoxide; dmap; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.051
Guidance literature:
Multi-step reaction with 6 steps
1: tert.-butyl lithium / tetrahydrofuran / -78 °C
2: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C
3: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C
4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
6: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C
With tert.-butylhydroperoxide; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.tetlet.2011.08.051
upstream raw materials:

C13H17NO4

C21H34O5Si

C29H42O6Si

C23H28O6

Downstream raw materials:

C39H46O6Si

C26H38O6Si

C29H45O9PSi

C29H43O9PSi

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