3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

Base Information

Chemical Name:3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline
CAS No.:1425037-34-8
Molecular Formula:C₂₄H₂₀F₆N₂
Molecular Weight:450.427
Hs Code.:

Synonyms:3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

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Chemical Property of 3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

Chemical Property:

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Technology Process of 3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

There total 4 articles about 3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59770-96-6,68120-41-2
1-(1-bromoethyl)-3-(trifluoromethyl)benzene

: 1425037-28-0
2-(3-trifluoromethyl-phenyl)-1,2,3,4-tetrahydroquinoxaline

: 1425037-34-8
3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1448-87-9
2-chloroquinoxaline

: 1425037-34-8
3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tetrahydrofuran; water / 75 °C / Inert atmosphere

2: borane-THF / tetrahydrofuran / 4 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; borane-THF; palladium diacetate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: 1423-26-3
(meta-(trifluoromethyl)phenyl)boronic acid

: 1425037-34-8
3-[3-(trifluoromethyl)phenyl]-1-{1-[3-(trifluoromethyl)phenyl]ethyl}-1,2,3,4-tetrahydroquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tetrahydrofuran; water / 75 °C / Inert atmosphere

2: borane-THF / tetrahydrofuran / 4 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; borane-THF; palladium diacetate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;