2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

Base Information

Chemical Name:2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester
CAS No.:1333393-19-3
Molecular Formula:C₄₈H₄₇NO₁₀
Molecular Weight:797.902
Hs Code.:

Synonyms:2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

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Chemical Property of 2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

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Technology Process of 2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

There total 2 articles about 2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: p-methylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1333393-19-3
2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

Guidance literature:: p-methylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-formamide; In dichloromethane; at -10 ℃; Molecular sieve;

N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester; In dichloromethane; at -10 ℃; for 6h; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/anie.201100076

Reference yield:

: 136497-85-3
N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester

: p-methylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

: 1333393-19-3
2,3-di-O-benzyl-4,6-O-benzylidene-D-galactopyranosyl Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine allyl ester

Guidance literature:: p-methylphenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; Molecular sieve;

N-(9-fluorenylmethoxycarbonyl)-L-serine allyl ester; In dichloromethane; at -10 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/anie.201100076