C₁₃H₉BrCl₂N₂O

Base Information

Chemical Name:C₁₃H₉BrCl₂N₂O
CAS No.:845752-07-0
Molecular Formula:C₁₃H₉BrCl₂N₂O
Molecular Weight:360.037
Hs Code.:

C<sub>13</sub>H<sub>9</sub>BrCl<sub>2</sub>N<sub>2</sub>O

Synonyms:C₁₃H₉BrCl₂N₂O

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Chemical Property of C₁₃H₉BrCl₂N₂O

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Technology Process of C₁₃H₉BrCl₂N₂O

There total 6 articles about C₁₃H₉BrCl₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 845752-07-0
C₁₃H₉BrCl₂N₂O

Guidance literature:: Multi-step reaction with 7 steps

1: phosphorus pentachloride; trichlorophosphate / 5 h / 70 - 140 °C

2: dipotassium hydrogenphosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide); water / 21 h / 68 °C

3: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C

4: bromine; acetic acid / 23 h / 20 °C

5: methanesulfonic acid / 130 °C

6: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

7: pyrrolidine / ethanol / 0.25 h

With pyrrolidine; hydrogenchloride; dipotassium hydrogenphosphate; methanesulfonic acid; phosphorus pentachloride; hydrogen; bromine; iron; acetic acid; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; water;

Reference yield:

: 845752-05-8
C₁₅H₁₀Br₂Cl₂N₂O₂

: 845752-07-0
C₁₃H₉BrCl₂N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

2: pyrrolidine / ethanol / 0.25 h

With pyrrolidine; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol;

Reference yield:

: 845752-03-6
C₁₁H₈Cl₂N₂

: 845752-07-0
C₁₃H₉BrCl₂N₂O

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; acetic acid / 23 h / 20 °C

2: methanesulfonic acid / 130 °C

3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 8 h / 20 °C

4: pyrrolidine / ethanol / 0.25 h

With pyrrolidine; methanesulfonic acid; hydrogen; bromine; acetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol;