C₄₁H₄₄O₆

Base Information

Chemical Name:C₄₁H₄₄O₆
CAS No.:1345718-84-4
Molecular Formula:C₄₁H₄₄O₆
Molecular Weight:632.797
Hs Code.:

C<sub>41</sub>H<sub>44</sub>O<sub>6</sub>

Synonyms:C₄₁H₄₄O₆

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Chemical Property of C₄₁H₄₄O₆

Chemical Property:

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Technology Process of C₄₁H₄₄O₆

There total 5 articles about C₄₁H₄₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 32437-88-0
6-<(tetrahydropyranyl)oxy>hexanoic acid

: 1345718-74-2
C₃₀H₂₆O₃

: 1345718-84-4
C₄₁H₄₄O₆

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1039/c1ob06047c

Reference yield:

: 105946-82-5
4-bromo-4'-iodobiphenyl

: 1345718-84-4
C₄₁H₄₄O₆

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere

3: potassium carbonate / methanol; dichloromethane / 3.5 h

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere

5: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling / 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1039/c1ob06047c

Reference yield:

: 1345718-66-2
C₁₅H₁₁BrO

: 1345718-84-4
C₄₁H₄₄O₆

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere

2: potassium carbonate / methanol; dichloromethane / 3.5 h

3: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere

4: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1039/c1ob06047c