{(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

Base Information

Chemical Name:{(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester
CAS No.:900798-78-9
Molecular Formula:C₄₂H₄₉N₃O₄
Molecular Weight:659.869
Hs Code.:

Synonyms:{(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

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Chemical Property of {(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

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Technology Process of {(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

There total 1 articles about {(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 900799-09-9
2-but-3-enyl-6-methyl-isonicotinic acid hydrochloride

: 900800-09-1
{(1S,2R)-1-(3-allyl-benzyl)-3-[benzyloxycarbonyl-(3-isopropyl-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester

: 900798-78-9
{(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

Guidance literature:: {(1S,2R)-1-(3-allyl-benzyl)-3-[benzyloxycarbonyl-(3-isopropyl-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid tert-butyl ester; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

2-but-3-enyl-6-methyl-isonicotinic acid hydrochloride; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 900798-78-9
{(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester

: 900798-01-8
(S)-4-[(R)-1-hydroxy-2-(3-isopropylbenzylamino)ethyl]-18-methyl-3,17-diazatricyclo[14.3.1.1*6,10*]henicosa-1⁽²⁰⁾,6,8,10⁽²¹⁾,16,18-hexaen-2-one

Guidance literature:: {(2R,3S)-4-(3-Allyl-phenyl)-3-[(2-but-3-enyl-6-methyl-pyridine-4-carbonyl)-amino]-2-hydroxy-butyl}-(3-isopropyl-benzyl)-carbamic acid benzyl ester; With hydrogenchloride; In 1,4-dioxane; dichloromethane; for 1h;

dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); In dichloromethane; for 72h; Heating / reflux;

With hydrogen; 5%-palladium/activated carbon; In methanol; at 20 ℃; for 9h; under 760.051 Torr;