N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

Base Information

Chemical Name:N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide
CAS No.:850148-19-5
Molecular Formula:C₂₃H₁₇ClN₄O₄S
Molecular Weight:480.931
Hs Code.:

Synonyms:N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

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Chemical Property of N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

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Technology Process of N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

There total 3 articles about N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 850148-18-4
(2-amino-5-acetic acid methyl ester sulfanyl-phenyl)-N-(5-chloro-(2-pyridyl))carboxamide

: 6068-72-0
4-cyanobenzoyl chlorIde

: 850148-19-5
N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

: 850148-17-3
N-(5-chloro-2-pyridinyl)-(2-nitro)-5-acetic acid methyl ester sulfanyl-phenylcarboxamide

: 850148-19-5
N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: tin(ll) chloride / ethyl acetate / 0.5 h / Heating / reflux

2: tetrahydrofuran / 0.5 h / 20 °C

With tin(ll) chloride; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 850148-19-5
N-(5-chloro-(2-pyridyl)){5-acetic acid methyl ester sufanyl-2-[(4-cyanophenyl)carbonylamino]phenyl}carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / pyridine / 0.5 h

2: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 50 °C

3: tin(ll) chloride / ethyl acetate / 0.5 h / Heating / reflux

4: tetrahydrofuran / 0.5 h / 20 °C

With caesium carbonate; tin(ll) chloride; trichlorophosphate; In tetrahydrofuran; pyridine; ethyl acetate; N,N-dimethyl-formamide;