2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium

Base Information

• Chemical Name: 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium
• CAS No.: 1092940-78-7
• Molecular Formula: C₆H₁₅N*C₃₁H₃₃N₉O₁₂S
• Molecular Weight: 856.914

Synonyms:2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium

Chemical Property of 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium

Chemical Property:

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Technology Process of 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium

There total 1 articles about 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N₆-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N-hydroxysuccinimidyl 2-(methoxymethyloxy)benzoate (918644-14-1) + 2-azido-2',3'-O-isopropylidene-5'-O-(sulfamoyl)adenosine (1092940-76-5) + triethylamine (121-44-8) → 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N6-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium (1092940-78-7)

Guidance literature:

N-hydroxysuccinimidyl 2-(methoxymethyloxy)benzoate; 2-azido-2',3'-O-isopropylidene-5'-O-(sulfamoyl)adenosine; With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

triethylamine;

DOI:10.1021/jm8008037

Reference yield:

2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}-N6-[2-(methoxymethoxy)benzoyl]adenosine triethylammonium (1092940-78-7) → 2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}adenosine triethylammonium (1092940-80-1)

Guidance literature:

With ammonia; In methanol; at 0 - 60 ℃; regioselective reaction; Inert atmosphere;

DOI:10.1021/jm8008037

upstream raw materials:

N-hydroxysuccinimidyl 2-(methoxymethyloxy)benzoate

2-azido-2',3'-O-isopropylidene-5'-O-(sulfamoyl)adenosine

triethylamine

Downstream raw materials:

2-azido-2',3'-O-isopropylidene-5'-O-{N-[2-(methoxymethoxy)benzoyl]sulfamoyl}adenosine triethylammonium

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