2-ETHYLCYCLOBUTANONE

Base Information

• Chemical Name: 2-ETHYLCYCLOBUTANONE
• CAS No.: 10374-14-8
• Molecular Formula: C6H10 O
• Molecular Weight: 98.143
• Hs Code.: 2914299000
• Mol file: 10374-14-8.mol

Synonyms:2-Ethylcyclobutanone

Chemical Property of 2-ETHYLCYCLOBUTANONE

Chemical Property:

• PSA: 17.07000
• LogP: 1.37550

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Ethylcyclobutanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-ETHYLCYCLOBUTANONE

There total 6 articles about 2-ETHYLCYCLOBUTANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

1-(1-Isopropoxy)propyl-1-cyclopropanol → 2-ethylcyclobutanone (10374-14-8)

Guidance literature:

With sulfuric acid; In diethyl ether; Heating;

Reference yield: 45.0%

1-<(phenylthio)cyclopropyl>-1-propanol (122540-25-4) → 2-ethylcyclobutanone (10374-14-8) + 1,1-di(phenylthio)-2-ethylcyclobutane (122732-87-0)

Guidance literature:

With hydrogen bromide; zinc dibromide; for 2h; Ambient temperature;

Reference yield:

m-Nitro-benzolsulfonsaeure- (17714-52-2) → 2-ethylcyclobutanone (10374-14-8)

Guidance literature:

With sodium 2,2,2-trifluoroacetate; In trifluoroacetic acid; at 50 ℃; for 120h;

upstream raw materials:

m-Nitro-benzolsulfonsaeure-

1-<(phenylthio)cyclopropyl>-1-propanol

3-Brom-2-acetoxy-cyclobuten-⁽¹⁾

ethylmagnesium bromide

Downstream raw materials:

2-ethyl-1-p-fluorophenyl-1-cyclobutanol

4-hydroxyhexanal

Refernces

• 1、 Hanack,Herterich. "". . p. 3847,3849. Retrieved 1966.
• 2、 Kwon, Tae Woo,Smith, Michael B.. "A Preparative Route to 2-Substituted 1,1-Diphenylthio Cyclobutanes". . p. 2027 - 2028. Retrieved 2007/10/02.