phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

Base Information

Chemical Name:phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside
CAS No.:848416-54-6
Molecular Formula:C₂₆H₂₈O₄S
Molecular Weight:436.572
Hs Code.:

Synonyms:phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

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Chemical Property of phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

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Technology Process of phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

There total 3 articles about phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 939-26-4
2-bromomethylnaphthyl bromide

: 196397-59-8
phenyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 848416-54-6
phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2004.11.056

Reference yield:

: 187233-24-5
phenyl 6-deoxy-1-thio-β-L-galactopyranoside

: 848416-54-6
phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / p-toluenesulfonic acid / 48 h / 20 °C

2: 96 percent / sodium hydride / dimethylformamide / 2 h / 20 °C

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.11.056

Reference yield:

: 127061-10-3
phenyl 2,3,4-tri-O-acetyl-1-thio-L-fucopyranoside

: 848416-54-6
phenyl 3,4-O-isopropylidene-2-O-(2-naphthyl)methyl-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / sodium methoxide / methanol / 20 °C

2: 89 percent / p-toluenesulfonic acid / 48 h / 20 °C

3: 96 percent / sodium hydride / dimethylformamide / 2 h / 20 °C

With sodium methylate; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.11.056