3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

Base Information

Chemical Name:3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate
CAS No.:1289374-95-3
Molecular Formula:C₂₀H₂₁N₃OS₂
Molecular Weight:383.538
Hs Code.:

Synonyms:3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

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Chemical Property of 3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

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Technology Process of 3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

There total 4 articles about 3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75-15-0,12122-00-8
carbon disulfide

: (E)-N-(3-butylbenzimidazol-3-ium-1-yl)-1-(4-methoxyphenyl)methanimine iodide

: 1289374-95-3
3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jo200088s

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1289374-95-3
3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; hydroxylamine-O-sulfonic acid / water / 3 h / 20 °C

2: sulfuric acid / ethanol / 5 h

3: 5 h / 100 °C

4: sodium hydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; potassium hydroxide; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo200088s

Reference yield:

: (E)-N-(benzimidazol-1-yl)-1-(4-methoxyphenyl)methanimine

: 1289374-95-3
3-butyl-1-[(E)-(4-methoxyphenyl)methyleneamino]benzimidazol-3-ium-2-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 5 h / 100 °C

2: sodium hydride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo200088s