5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

Base Information

Chemical Name:5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one
CAS No.:1326305-17-2
Molecular Formula:C₁₅H₁₅ClN₄O
Molecular Weight:302.763
Hs Code.:

Synonyms:5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

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Chemical Property of 5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

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Technology Process of 5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

There total 6 articles about 5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 587-04-2
m-Chlorobenzaldehyde

: 139756-02-8
4-amino-1-methyl-3-propyl-1H-pyrazole-5-carboxamide

: 1326305-17-2
5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

Guidance literature:: With dipotassium peroxodisulfate; In water; dimethyl sulfoxide; at 100 ℃; Sealed tube; Microwave irradiation;
DOI:10.1016/j.ejmech.2014.04.051

Reference yield:

: 92945-27-2
ethyl 3-propyl-1H-pyrazole-5-carboxylate

: 1326305-17-2
5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

Guidance literature:: Multi-step reaction with 6 steps

1.1: 9 h / 5 - 25 °C

2.1: sodium hydroxide / 3 h / 75 °C

3.1: sulfuric acid; nitric acid / 8 h / 50 °C

4.1: thionyl chloride / 5 h / Reflux

5.1: iron; ammonium chloride / ethanol; water / 4.5 h / 80 °C

6.1: ethanol / 1.5 h / 75 °C

6.2: 1.5 h / 75 °C

With thionyl chloride; sulfuric acid; nitric acid; iron; ammonium chloride; sodium hydroxide; In ethanol; water;

Reference yield:

: 133261-07-1
1-Methyl-3-n-propylpyrazole-5-carboxylic acid ethyl ester

: 1326305-17-2
5-(3-chlorophenyl)-1-methyl-3-propyl-1H-pyrazolo[4,3-d]pyrimidin-7(6H)-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / 3 h / 75 °C

2.1: sulfuric acid; nitric acid / 8 h / 50 °C

3.1: thionyl chloride / 5 h / Reflux

4.1: iron; ammonium chloride / ethanol; water / 4.5 h / 80 °C

5.1: ethanol / 1.5 h / 75 °C

5.2: 1.5 h / 75 °C

With thionyl chloride; sulfuric acid; nitric acid; iron; ammonium chloride; sodium hydroxide; In ethanol; water;