1,3-Dichloro-1,3-diethyldialuminoxane

Base Information

Chemical Name:1,3-Dichloro-1,3-diethyldialuminoxane
CAS No.:10301-15-2
Molecular Formula:C₄H₁₀Al₂Cl₂O
Molecular Weight:198.992
Hs Code.:
DSSTox Substance ID:DTXSID50586829
Wikidata:Q82479038
Mol file:10301-15-2.mol

Synonyms:10301-15-2;chloro-[chloro(ethyl)alumanyl]oxy-ethylalumane;1,3-Dichloro-1,3-diethyldialuminoxane;SCHEMBL5048736;DTXSID50586829

Suppliers and Price of 1,3-Dichloro-1,3-diethyldialuminoxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1,3-Dichloro-1,3-diethyldialuminoxane

Chemical Property:

Boiling Point:111 °C
Flash Point:12 °F
PSA：9.23000
Density:0.885 g/mL at 25 °C
LogP:-3.70050
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:197.973947
Heavy Atom Count:9
Complexity:65.6

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:F,T
Statements: 11-14-23/24/25-34
Safety Statements: 16-26-36/37/39-43-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Al](O[Al](CC)Cl)Cl

Technology Process of 1,3-Dichloro-1,3-diethyldialuminoxane

There total 13 articles about 1,3-Dichloro-1,3-diethyldialuminoxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13477-89-9
neodymium(III) chloride hexahydrate

: 563-43-9
ethylaluminum dichloride

: NdCl₃*0.5H₂O*0.5((C₂H₅)AlCl)2O

: 10301-15-2
1.3-Diethyl-1.3-dichlor-alumoxan

Guidance literature:: In toluene; Petroleum ether; byproducts: HCl, C2H6; (Ar); using Schlenk techniques; addn. of soln. of (C2H5)AlCl2 (12 equiv.) in petroleum ether to stirred suspn. of NdCl3*6H2O (1 equiv.) in toluene for 20 min at 40, 50, 70 and 90°C; stirring for 10 min; pptn., filtration, washing of solid twice with toluene and drying under vac., removal of solvent from filtrate in vac., elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(01)01166-4

Reference yield:

: dysprosium(III) chloride hexahydrate

: 563-43-9
ethylaluminum dichloride

: DyCl₃*0.5H₂O*0.5((C₂H₅)AlCl)2O

: 10301-15-2
1.3-Diethyl-1.3-dichlor-alumoxan

Guidance literature:: In toluene; Petroleum ether; byproducts: C2H6, HCl; (Ar); using Schlenk techniques; addn. of soln. of (C2H5)AlCl2 (12 equiv.) in petroleum ether to stirred suspn. of DyCl3*6H2O (1 equiv.) in toluene for 20 min at 40, 50, 70 and 90°C; stirring for 10 min; pptn., filtration, washing of solid twice with toluene and drying under vac., removal of solvent from filtrate in vac., elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(01)01166-4

Reference yield:

: 13798-24-8,19423-82-6
terbium(III) chloride hexahydrate

: 563-43-9
ethylaluminum dichloride

: TbCl₃*0.5H₂O*0.5((C₂H₅)AlCl)2O

: 10301-15-2
1.3-Diethyl-1.3-dichlor-alumoxan

Guidance literature:: In toluene; Petroleum ether; byproducts: HCl, C2H6; (Ar); using Schlenk techniques; addn. of soln. of (C2H5)AlCl2 (12 equiv.) in petroleum ether to stirred suspn. of TbCl3*6H2O (1 equiv.) in toluene for 20 min at 40, 50, 70 and 90°C; stirring for 10 min; pptn., filtration, washing of solid twice with toluene and drying under vac., removal of solvent from filtrate in vac., elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(01)01166-4