methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

Base Information

Chemical Name:methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside
CAS No.:93960-45-3
Molecular Formula:C₂₉H₃₁FO₅
Molecular Weight:478.561
Hs Code.:

Synonyms:methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

There total 4 articles about methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 93960-43-1
methyl-3,4-O-isopropylidene-2-O-(trifluoromethanesulfonyl)-6-O-trityl-β-D-talopyranoside

: 93960-45-3
methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

Guidance literature:: With tetraethylammonium fluoride; In acetonitrile; at 50 ℃; for 0.833333h;

Reference yield:

: 34698-24-3
methyl 3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

: 93960-45-3
methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: DMSO / acetic anhydride

2: lithium aluminum hydride

3: pyridine

4: 50 percent / tetraethylammonium fluoride / acetonitrile / 0.83 h / 50 °C

With lithium aluminium tetrahydride; tetraethylammonium fluoride; dimethyl sulfoxide; In pyridine; acetic anhydride; acetonitrile;

Reference yield:

: 66295-15-6
(3aS,4R,6R,7aS)-6-Methoxy-2,2-dimethyl-4-trityloxymethyl-dihydro-[1,3]dioxolo[4,5-c]pyran-7-one

: 93960-45-3
methyl 2-deoxy-2-fluoro-3,4-O-isopropylidene-6-O-trityl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride

2: pyridine

3: 50 percent / tetraethylammonium fluoride / acetonitrile / 0.83 h / 50 °C

With lithium aluminium tetrahydride; tetraethylammonium fluoride; In pyridine; acetonitrile;