C₂₂H₂₈N₂O

Base Information

Chemical Name:C₂₂H₂₈N₂O
CAS No.:1278575-08-8
Molecular Formula:C₂₂H₂₈N₂O
Molecular Weight:336.477
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>2</sub>O

Synonyms:C₂₂H₂₈N₂O

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Chemical Property of C₂₂H₂₈N₂O

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Technology Process of C₂₂H₂₈N₂O

There total 4 articles about C₂₂H₂₈N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1278574-96-1
C₂₂H₂₆N₂O₃

: 1278575-08-8
C₂₂H₂₈N₂O

Guidance literature:: With hydrogenchloride; acetic acid; zinc; In methanol; water; at 20 ℃; for 3h;
DOI:10.1021/jo1025833

Reference yield:

: 120-72-9
indole

: 1278575-08-8
C₂₂H₂₈N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol / toluene / 20 °C / Inert atmosphere

2: hydrogenchloride; acetic acid; zinc / methanol; water / 3 h / 20 °C

With hydrogenchloride; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol; 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; acetic acid; zinc; In methanol; water; toluene; 1: Friedel Crafts/Henry reaction;
DOI:10.1021/jo1025833

Reference yield:

: 150367-10-5,78346-64-2
1-nitro-1-heptene

: 1278575-08-8
C₂₂H₂₈N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol / toluene / 20 °C / Inert atmosphere

2: hydrogenchloride; acetic acid; zinc / methanol; water / 3 h / 20 °C

With hydrogenchloride; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol; 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; acetic acid; zinc; In methanol; water; toluene; 1: Friedel Crafts/Henry reaction;
DOI:10.1021/jo1025833