DB₃₀C₁₀DE

Base Information

• Chemical Name: DB₃₀C₁₀DE
• CAS No.: 1207666-07-6
• Molecular Formula: C₄₈H₅₂O₁₄
• Molecular Weight: 852.932
• Mol file: 1207666-07-6.mol

Synonyms:DB₃₀C₁₀DE

Chemical Property of DB₃₀C₁₀DE

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DB₃₀C₁₀DE

There total 2 articles about DB₃₀C₁₀DE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C28H38I2O10 (1207665-99-3) + 4-ethynylbenzoic acid methyl ester (3034-86-4) → DB30C10DE (1207666-07-6)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; diisopropylamine; triphenylphosphine; In tetrahydrofuran; at 80 ℃; for 8h; Inert atmosphere;

DOI:10.1002/chem.200902350

Reference yield: 16.0%

C26H18O6 (1207665-97-1) + C36H50O14S2 (448236-29-1) → DB30C10DE (1207666-07-6)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 53h; Inert atmosphere;

DOI:10.1002/chem.200902350

Reference yield: 91.0%

DB30C10DE (1207666-07-6) → DB30C10DA (1207666-08-7)

Guidance literature:

DB₃₀C₁₀DE; With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; water;

DOI:10.1002/chem.200902350

upstream raw materials:

C₂₆H₁₈O₆

C₃₆H₅₀O₁₄S₂

C₂₈H₃₈I₂O₁₀

4-ethynylbenzoic acid methyl ester

Downstream raw materials:

DB₃₀C₁₀DA