3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one

Base Information

• Chemical Name: 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one
• CAS No.: 110450-75-4
• Molecular Formula: C₃₄H₄₀O₁₃
• Molecular Weight: 656.684

Synonyms:3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one

Chemical Property of 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one

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Technology Process of 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one

There total 2 articles about 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(E)-3-{4-Hydroxy-3-[(E)-3-(3-methoxy-4-methoxymethoxy-phenyl)-allyloxy]-phenyl}-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone (134037-02-8) → 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.03,7]dec-8-en-2-one (110450-75-4)

Guidance literature:

With lithium perchlorate; In tetrahydrofuran; methanol; anodic oxidation;

DOI:10.1016/S0040-4020(01)87053-8

Reference yield:

2,4,6-tri-MOM phloracetophenone (36804-11-2) → 3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.03,7]dec-8-en-2-one (110450-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Triton B, 2.) nBu₄NF / 1.) benzene, MeOH, 24 h, room temperature, 2.) THF, 45 deg C, 20 h

2: 82 percent / LiClO₄ / methanol; tetrahydrofuran / anodic oxidation

With tetrabutyl ammonium fluoride; lithium perchlorate; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4020(01)87053-8

Reference yield:

3-Methoxy-10-(3-methoxy-4-methoxymethoxy-phenyl)-8-[(E)-3-oxo-3-(2,4,6-tris-methoxymethoxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.03,7]dec-8-en-2-one (110450-75-4) → 10-(4-Hydroxy-3-methoxy-phenyl)-3-methoxy-8-[(E)-3-oxo-3-(2,4,6-trihydroxy-phenyl)-propenyl]-4-oxa-tricyclo[4.3.1.03,7]dec-8-en-2-one

Guidance literature:

With hydrogenchloride; In methanol; for 0.0833333h; Heating;

DOI:10.1016/S0040-4020(01)87053-8

upstream raw materials:

(E)-3-{4-Hydroxy-3-[(E)-3-(3-methoxy-4-methoxymethoxy-phenyl)-allyloxy]-phenyl}-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

2,4,6-tri-MOM phloracetophenone

Downstream raw materials:

8-(5,7-Dihydroxy-4-oxo-chroman-2-yl)-10-(4-hydroxy-3-methoxy-phenyl)-3-methoxy-4-oxa-tricyclo[4.3.1.0^3,7]dec-8-en-2-one

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