(3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate

Base Information

• Chemical Name: (3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate
• CAS No.: 1027785-39-2
• Molecular Formula: C₆₈H₈₃N₃O₇S₂Si
• Molecular Weight: 1146.64

Synonyms:(3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate

Chemical Property of (3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate

Chemical Property:

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Technology Process of (3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate

There total 1 articles about (3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(3S,4R,5R)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate (1027785-37-0) → (3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate (1027785-39-2)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 3h;

DOI:10.1039/b718310k

Reference yield: 99.0%

(3S,4R,5S)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate (1027785-39-2) → (3S,4R,5S)-3-(tert-Butyldimethylsiloxy)-4-{(S)-2-[(R)-2-[(S,E)-3-(4-methoxybenzyloxy)-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino}-5-methylheptanoic acid (1027785-41-6)

Guidance literature:

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1039/b718310k

upstream raw materials:

(3S,4R,5R)-allyl 3-(tert-butyldimethylsiloxy)-4-[(S)-2-[(R)-2-[(S,E)-3-hydroxy-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino]-5-methylheptanoate

Downstream raw materials:

(3S,4R,5S)-3-(tert-Butyldimethylsiloxy)-4-{(S)-2-[(R)-2-[(S,E)-3-(4-methoxybenzyloxy)-7-(tritylthio)hept-4-enoylamino]propionylamino]-3-(tritylthio)propionylamino}-5-methylheptanoic acid

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