2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

Base Information

Chemical Name:2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene
CAS No.:76799-64-9
Molecular Formula:C₁₄H₁₈O₈
Molecular Weight:314.292
Hs Code.:

Synonyms:2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

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Technology Process of 2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

There total 2 articles about 2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 76799-18-3
2-<3-(benzyloxy)-4-methoxyphenyl>-6-(benzyloxy)-7α,8β-dihydroxy-1,3,5-trioxatetrahydronaphthalene

: 76799-64-9
2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water; for 24h; under 2280 Torr; Ambient temperature;
DOI:10.1021/jm00136a011

Reference yield:

: 76799-17-2
3-(benzyloxy)-4-methoxybenzaldehyde dimethyl acetal

: 76799-64-9
2-(3-hydroxy-4-methoxyphenyl)-6,7α,8β-trihydroxy-1,3,5-trioxatetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / p-TsOH / benzene; dioxane / Ambient temperature

2: 92 percent / H₂ / Pd/C / tetrahydrofuran; methanol; H₂O / 24 h / 2280 Torr / Ambient temperature

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; water; benzene;
DOI:10.1021/jm00136a011